Total Lab Supplies - Everything for your laboratory

Total Lab Supplies - Everything for your laboratory
Our Head Office in St Helens
Showing posts with label hotplate stirrer. Show all posts
Showing posts with label hotplate stirrer. Show all posts

Friday, 22 February 2019

Hotplate Safety

Total Lab Supplies offer a wide range of hotplates and hotplate/stirrers.  The Stuart range is well known in laboratories and they offer some good advice on the operation of these units.

  • Do not use hotplates to heat inflammable liquids.
  • Never lift or carry a hotplate until it has been switched off and allowed to cool for at least 30 minutes. A hot warning light will give guidance.
  • A hotplate should be carried using both hands with the fingers under the side edges.
  • Never move or carry a unit with containers on the top plate or while still connected to the mains supply.
  • There is a danger of liquid spillage if containers are over-filled and stirred at high speed. Always build stirrer speed slowly and never stir more rapidly than necessary
  • NEVER place a cold glass vessel onto a hotplate which is already hot.

When using a ceramic hotplates like the Stuart UC152 at temperatures over 180ÂșC, the base of any equipment used must not make contact with the ceramic plate outside the Hot Zone or heated plate area.

The use of a Stuart SCT1 temperature controller allows accurate temperature control of aqueous and oil based samples in the laboratory and can be used in two different modes, as a precise temperature controller from 20 to 200°C or as a digital thermometer from -4 to 325°C.

Care when preparing media
Take particular care when heating liquids having a high viscosity. Viscous liquids can act as thermal insulators and can cause thermal breakage of the glassware. This is very important with media solutions as the viscosity will usually increase as the temperature rises.

  • Check that the stirring action is sufficient to agitate the whole of the liquid.  Unstirred areas in the liquid can result in uneven heat transfer and “hot spots” in the glassware. This can induce thermal stress and so cause failure.
  • Check the stirring action regularly to ensure that it remains adequate as the viscosity of the solution increases.
  • Always use the largest magnetic follower possible and if necessary, use a mechanical overhead stirrer.
  • Do not use glass vessels with thick walls, e.g. Pyrex Heavy Duty Ware or standard beakers and flasks having capacities of 5 litres or greater.
  • NEVER heat glass bottles on a hotplate.
  • Ensure that the heat is built up slowly to avoid localised overheating.
  • Ensure the glassware is completely free from scratches or other defects.
  • Place the hotplate in a tray large enough to contain the liquid in the event of glassware failure.
  • Wear the appropriate safety clothing e.g. gloves, goggles, protective apron etc.

Following these guidelines using a stirrer/hotplate should ensure trouble free use.

 For all your hotplate/stirrer needs please get in touch

Friday, 29 November 2013

The Magnetic Stirrer


A magnetic stirrer is a piece of laboratory equipment that uses a rotating magnetic field to cause a stirrer bar (also called "flea") immersed in a liquid to spin very quickly, thus stirring it.  The rotating field may be created either by a rotating magnet or a set of stationary electromagnets, placed beneath the vessel with the liquid.

Glass does not affect a magnetic field and most chemical reactions take place in glass vessels (i.e. beakers or flasks) and magnetic stirrer bars work well in glass vessels. However, the limited size of the bar means that magnetic stirrers can only be used for relatively small (under 4 litres) experiments.  They also have difficulty dealing with viscous liquids or thick suspensions.  For larger volumes or more viscous liquids, some sort of mechanical stirring is typically needed.

Ika C-MAG HS 7
 
Magnetic stirrers are preferred over gear-driven motorized stirrers because they are quieter, more efficient, and have no moving external parts to break or wear out (other than the simple bar magnet itself).  Due to its small size, a stirrer bar is more easily cleaned and sterilised than other stirring devices.  They do not require lubricants which could contaminate the reaction vessel and the product. They can be used inside hermetically closed vessels or systems, without the need for complicated rotary seals. Magnetic stirrers may also include a heating element to heat the liquid being stirred.

Arthur Rosinger of Newark, New Jersey, U.S.A. obtained US Patent 2,350,534, titled Magnetic Stirrer on 6 June 1944, having filed an application on 5 October 1942.   His patent includes a description of a coated bar magnet placed in a vessel, which is driven by a rotating magnet in a base below the vessel. His patent explains that coating the magnet in plastic or covering it with glass or porcelain makes it chemically inert.

The plastic-coated bar magnet was independently invented in the late 1940s by Edward McLaughlin, of the Torpedo Experimental Establishment (TEE), Greenock, Scotland, who named it the 'flea' because of the way it jumps about if the rotating magnet is driven too fast.

An even earlier patent for a magnetic mixer is US 1,242,493, issued 9 October 1917 to Richard H. Stringham of Bountiful, Utah, U.S.A. Mr. Stringman's mixer used stationary electromagnets in the base, rather than a rotating permanent magnet, to rotate the stirrer.

For more information visit:-
http://en.wikipedia.org/wiki/Magnetic_stirrer
http://www.prlabs.co.uk
http://www.prlabs.co.uk/news/article.php?Id=125