Desiccator |
The contents of desiccators are exposed to atmospheric moisture whenever the desiccators are opened. It also requires some time to achieve a low humidity. Hence they are not appropriate for storing chemicals which react quickly or violently with atmospheric moisture such as the alkali metals.
The lower compartment of the desiccator contains lumps of freshly calcined quicklime or (not as effective) calcined calcium chloride to absorb water vapours. The substance is put in the upper compartment (on the porcelain plate). The ground-glass rim of the desiccator lid must be thoroughly greased with a thin layer of petroleum jelly melted together with beeswax or paraffin wax.
In order to open the desiccator without damage, remove the lid sideways horizontally not to upwards. Cover the desiccator in the same way.
In laboratory use, the most common desiccators are circular and made of heavy glass. There is usually a removable platform on which the items to be stored are placed. The desiccant, usually an otherwise-inert solid such as silica gel, fills the space under the platform.
A stopcock may be included to permit the desiccator to be evacuated. Such models are usually known as vacuum desiccators. When a vacuum is to be applied, it is a common practice to criss-cross the vacuum desiccator with tape, or to place it behind a screen to minimize damage or injury caused by an implosion. To maintain a good seal, vacuum grease is usually applied to the flanges.
Visit http://www.prlabs.co.uk for more information or:-
http://en.wikipedia.org/wiki/Dessicator
http://www.scilabware.com/Desiccators/Non-vacuum-desiccators/p-48-197/
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